Nanoactivated carbon synthesized by thermal treatment (Flow-N2) over lignocellulosic wastes from cocoa pod husk applied in removal

Authors

DOI:

https://doi.org/10.61117/ipsumtec.v8i1.360

Keywords:

bioadsorbent nanomaterials, environmental impact, waste management, remotion, aqueous pollutants, lignocellulosic wastes

Abstract

Nanomaterials, that is, materials on a nanometric scale, with dimensions less than 100 nm, using lignocellulosic waste (residual biomass) as raw material for synthesis, are a sustainable alternative, which contributes to the principles of green chemistry and the circular economy. The synthesis method used is based on a delignification process, promoted by pyrolysis, for this, a Nabertherm brand tubular muffle with a quartz tube was used. The process was carried out at temperatures of 500°C and 700°C for 1 or 2 hours in the presence of N2 flow, using a Proportional Integral Derivative (PID) controller, which generated Nano Activated Carbon (NCA), from cocoa shell.

Eutrophic systems resulting from poor management of domestic wastewater include negative consequences such

as human health, destruction of aquatic ecosystems and deterioration in water quality for human consumption. That is why we tested our NAC in liquid samples taken from Laguna de las Ilusiones, considered a Protected Natural Area of ​​our State, to test the capacity of synthesized bioadsorbent nanomaterials contributing to efficient, modern, and low-cost technologies in the elimination of contaminants in real systems.

The adsorption experiments were carried out under conditions of 30 °C, reaching an efficient 70% removal. Furthermore, compared to materials treated with chemical agents, these reached 70% but with more severe conditions of 35°C. Therefore, the improvement in the economy of the process was achieved with the NAC synthesized by thermal treatment.

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Author Biographies

Zenaida Guerra Que , National Technological Institute of Mexico

Recognized researcher in the field of nanomaterial sciences. She actively participates in the dissemination of sustainable practices and development of innovative technological solutions using nanotechnology for the care of the environment. She is a full time professor at the Tecnológico Nacional de México-Instituto Tecnológico de Villahermosa. Her scientific production includes more than 10 publications in journals indexed in the Journal Citation Report, 7 refereed articles with ISSN, 5 book chapters with ISBN. She has been promoted to Level 1 in the SNII of SECIHTI.

Kristal de María Jesús de la Cruz , National Technological Institute of Mexico

D. in Ecology and Management of Tropical Systems, graduated from the Academic Division of Biological Sciences (DACBIOL), Universidad Juárez Autónoma de Tabasco (UJAT). Master of Science in Biochemical Engineering and Bachelor of Science in Biochemical Engineering/Instituto Tecnológico de Villahermosa (ITVH), Professor with current Desirable Profile in the Dept. of Chemistry, Biochemistry and Environment of the Instituto Tecnológico de Villahermosa (ITVH).

Hortensia Eliseo Dantés, National Technological Institute of Mexico

D. in Management Sciences is a full time professor at the Tecnológico Nacional de México. Instituto Tecnológico de Villahermosa, she is an Industrial Engineer in Career Production and holds a Master's Degree in Business Planning and Regional Development. She is dedicated to research in the Social Sciences with integral orientation to the solution of problems in the field of Productivity and Competitiveness, as well as sustainability. She belongs to the National System of Researchers (SNII) Candidate level.

Adib Abiu Silahua Pavón , National Technological Institute of Mexico

D. in Materials Sciences from the Universidad Juárez Autónoma de Tabasco. Professor at the Instituto Tecnológico de Villahermosa-TECNM in the Department of Earth Sciences. Currently, he belongs to the National System of Researchers (SNII) Level 1. His line of expertise is the design of nanostructured catalysts applied to environmental remediation in the treatment of emerging pollutants and the production of biofuels from lignocellulosic waste.

Pedro García Alamilla, Universidad Juárez Autónoma de Tabasco

D. in Food Science and Engineering. Full-time professor of Food Engineering since 2007 to date, Basic Academic Core of the Master in Agri-Food Sciences and PhD in Agricultural Sciences of the Academic Division of Agricultural Sciences (DACA) of the Universidad Juárez Autónoma de Tabasco (UJAT). His specialty covers cocoa-chocolate transformation processes and the use of agri-food residues. She is currently a member of the National System of Researchers (SNII) level 1.

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2025-05-22

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Guerra Que , Z., Jesús de la Cruz , K. de M., Eliseo Dantés, H., Silahua Pavón , A. A., & García Alamilla, P. (2025). Nanoactivated carbon synthesized by thermal treatment (Flow-N2) over lignocellulosic wastes from cocoa pod husk applied in removal. REVISTA IPSUMTEC, 8(1), 64–74. https://doi.org/10.61117/ipsumtec.v8i1.360

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